How to Perform a Recrystallization ?
Answers were Sorted based on User's Feedback
Answer / taksena gurung
1 First choose a proper solvent to dissolve the impure
substance. the solvent should be like that, in cold
condition the substance is insoluble or partially soluble,
and in hot condition the substance should be completely
soluble.
2 After selecting the suitable solvent, dissolve the given
substance in it, and heat it till the substance completly
dissolve forming clear solution.
3 now filter this hot solution immediatly through the
filter paper. the insoluble impurity remains on the filter
paper and collect the filtrate in a dish and allow to cool
without disturbng the container.
4 the filtrate on cooling gives crystals which are pure,
homogenous, and bigger in size.
| Is This Answer Correct ? | 33 Yes | 0 No |
Answer / bhavin mehta
Recrystallization is a laboratory technique used to purify
solids based on their different solubilities.
Recrystallization Steps are
1)Add a small quantity of appropriate solvent to an impure
solid.
2)Apply heat to dissolve the solid.
3)Cool the solution to crystallize the product.
4)Use vacuum fitration to isolate and dry the purified
solid.
| Is This Answer Correct ? | 10 Yes | 5 No |
Answer / dinesh gurav
Recrystallisation is a crystallisation process of impure or
crude solid materials in different solvents and at diff.
experimental parameters like temp,pH and quantity of
solvents to elute out the unwanted compounds
[Impurities,Polymorphs] to get a compound of desired
quality.
| Is This Answer Correct ? | 4 Yes | 2 No |
Answer / tulasi
if compoune is dissolved in acid
then we have to add base and viceversa
| Is This Answer Correct ? | 1 Yes | 9 No |
how will you do the prep for unstable componds?
0 Answers AMRI, CTX Life Sciences, Piramal Healthcare,
how require to set assay concentration for standard and sample?
why sucrose is used for polarimeter calibration
What is the solvent/material used to balance spirit level in analytical balance?
5 Answers Glenmark, MMC Health Care,
Loss of linearity in tkn analysis, possible reasons?
if the flow rate is increases then any changes in retention time in hplc
why we are used 4,7,9,2 buffers for the ph calibration
4 Answers Aurobindo, Enaltec Labs,
What is the difference between Discriminating media and DPDM(Dissolution Profile with Different Media)
As per OOT for any product what is calculation and how to invetigate the OOT
Why Holium cholorate used in UV Spectro photometer?
Why the same type of columns showing different RT for a single product?
Why we check moisture,ash & AIA in product