Golgappa.net | Golgappa.org | BagIndia.net | BodyIndia.Com | CabIndia.net | CarsBikes.net | CarsBikes.org | CashIndia.net | ConsumerIndia.net | CookingIndia.net | DataIndia.net | DealIndia.net | EmailIndia.net | FirstTablet.com | FirstTourist.com | ForsaleIndia.net | IndiaBody.Com | IndiaCab.net | IndiaCash.net | IndiaModel.net | KidForum.net | OfficeIndia.net | PaysIndia.com | RestaurantIndia.net | RestaurantsIndia.net | SaleForum.net | SellForum.net | SoldIndia.com | StarIndia.net | TomatoCab.com | TomatoCabs.com | TownIndia.com
Interested to Buy Any Domain ? << Click Here >> for more details...


How to determine water content of thioanisole? which
interfere by KF titration?



How to determine water content of thioanisole? which interfere by KF titration?..

Answer / ashok babu jha

Procedure:
30 mL methanol +3 g imidazole +1g N-
Ethylmaleinimide . Titrte to dryness , add approx.03 g
sample from a dry syringe without needle , allow to react
under stirring for 5 min and then titrate the water content
with KF reagent.Ethylmaleinimide form covalent bonds with
sulfhydryl groups at pH 6.5-7.5 .

Is This Answer Correct ?    3 Yes 1 No

Post New Answer

More Analytical Chemistry Interview Questions

Shall i use a same hplc column for two different products.?

3 Answers  


which batch require to use for analytical method validation?

0 Answers  


why using factor 1.00639 in burette calibration of kf

1 Answers   Cipla,


What is column dead volume?

4 Answers   Astron Research,


who is the father of HPLC?

6 Answers   Cipla, IPCA,


What is the difference between Chromatograhic Purity And Related substances

11 Answers   Cipla,


why use benzophenone & caffene acetone in hplc calibration

1 Answers  


During Validation study, Recovery is passing at all levels but Linearity is failing. Justify?

1 Answers   Mylan, Torrent Pharma,


how peak can be sharp in hplc when it is come flat

6 Answers   Graviti Pharmaceuticals,


if the flow rate is increases then any changes in retention time in hplc

1 Answers  


How you start the method development of unknown compound.

1 Answers  


function of detecter in hplc ,gc and spectroscopy? function of carrier gas in gc?

0 Answers   DRL,


Categories
  • Organic Chemistry Interview Questions Organic Chemistry (342)
  • Inorganic Chemistry Interview Questions Inorganic Chemistry (123)
  • Analytical Chemistry Interview Questions Analytical Chemistry (1387)
  • Physical Chemistry Interview Questions Physical Chemistry (62)
  • General Chemistry Interview Questions General Chemistry (478)
  • Chemistry AllOther Interview Questions Chemistry AllOther (190)