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Why karl fisher factor is 5 ?
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Because 1ml of Kf reagent will nuetrlizes the minimum 5mg of water thats y kf factor is between 5-7 mg/ml
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If mass balance is not passing in forced degradation in method validation that method is suitable or not?
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In BP2013, Loperamid HCl monograph. Assay by titration with 0.1N sodium hydroxide using hydrocloric acid 0.01N and reading the volume added between the 2 points of inflexion. I have a question that if the diluent solvent is ethanol is certainly consumed a amount of volume of titrant, so this volume must be eliminated on the result calculation or not apart from first point which is subtracted above.
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