Why Dissolving and then reforming crystals can improve
their purity?
Answers were Sorted based on User's Feedback
Answer / obuli
The basic recrystallization plan is to dissolve an impure
solid in ahot solvent, then cool the solution so that the
desired molecules recrystallize while the
impurities remain in solution. Subsequent filtration
separates the solid crystal from the liquid
solvent.temperature (so that the impurities are freed), but
weak enough so that at least some of your
sample crystallizes out after cooling (so that you get at
least some yield harvested.)
Is This Answer Correct ? | 10 Yes | 2 No |
Answer / naveen gutta
Crystallization is a technique used to produce the purified form of the compound. Generally the purified form and the impurities will show different solubility characteristics in different solvents at different temperatures.Some compounds will dissolve at room temperature only and it can be recrystallized at a temperature less than RT. Usage of combination of two solvents (miscible/miscible depending on the solubility) is preferable for crystallization purpose.
Is This Answer Correct ? | 1 Yes | 1 No |
Is benzene aromatic?
Difference between calibration and validation
2 Answers Cipla, Zydus Cadila,
Trimethylamine is a pyramidal molecule. What is the hybridization at nitrogen?
Explain What is a base line in GC and HPLC?
i am serching new job please help me
Why some type of assays having limit 98% to102%? (if any compound having assay limit 100)
3 Answers Asia Pharma, Reddy Labs,
Suppose we prepared pH buffer solution in lab.and calibrate against NIST solution, and same shall going to used upto 30 days. is it possible to stable pH and appearance? suggest?
2+2 CYCLO ADDITION OPTICALLY ACTIVE OR THERMALLY ACTIVE.
whenever kf titration is done that time one result is high and second one lower results what to do.
2 Answers Invochem Laboratory, Laurus,
what is a primary standard? what is a secondary standard solutions?
1 Answers Practical Viva Questions,
In describing structure of benzene, by molecular orbital treatment, either MOT or VBT explains its structure?
what are the differences between assay procedures and estimation in chemical analysis? also what is the equivalent factor that we consider in assay analytical procedures?
0 Answers Karnataka College of Pharmacy,