for heavy metal test lead used in which form pure form or any other form for preparation of lead standard sol
1 5315we run the same sample in same method in different flow rates in HPLC,any changes in sample analysis?
2 6588For limit test of heavy metals in BP, Method C require that the substance is ignited at a temperature not exceeding 800 °C. Why confines such the temperature?
3502For titration in anhydrous media with perchloric acide, if lack of titrator, Which indicator is been used for replacement. How calculate pH of test solution to choose suitable indicator?
1798stability study is going on up to 3years for famotidine-USP but the pharmacopeia is revised and tlc test is replaced with hplc test. At the 4th year frequency the product is failed in hplc test .how can i assain the expiry or retest date and can i stop or continue the programme?
2 5703Post New Analytical Chemistry Questions
What is the formula for relative diffrence for standard solution in solution stability in validation?
Identify problem faced when mass spectroscopy is used with HPLC system ?
what is diffrence between specificity and selecivity?
what is turbidimetric titration?Give 2 examples.
what is impurity profile. how to interpret this impurity profile to a drug product or drug substance.
why lactose has less charges when packed in steel containers when compared with packing of lactose in polyamide material?
inhouse product is in capsule form in combination and RLD is in tablet form then can we proceed for multimedia CDP? in inhouse capsule product disso is paddle with sinker in release media is there then RLD product in tablet form then with same as paddle with sinker we can proceed n.a.?
why xterra column require to use at higher ph?
IS THERE ANY EQUIPMENT TO CHECK AND CALCULATE THE POLARITY OF A LIQUID?
how to qualify the impurity?
if content uniformity passing but dissolution varrying then what is next step?
What is the accrptance criteria in RSD for RS method precision on basis of impurity percentages?
AT WHAT CONDITIONS WILL YOU ANALYSE A SAMPLE,WHICH ARE PRESERVED AT OTHER THAN THE AMBIENT CONDITIONS?(ie COLD STORAGE SAMPLES BELOW 20* CENTIGRADE?
why require the ph, buffer during hplc mobile phase?
What is related substance by HPLC impurity limits as per USP?