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Answer Posted / anutetakala
is there any moisture content testing by kf reagent for raw materials
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if identification threshold crosses the limits then what next step?
what are the guidelines for analytical method validations?
How do we fix the sample concentaryion in hplc method development. What is the basis?
In IR spectra, generally a molecule vibrates without apply emr or ir light?
in hplc chromatogram started from left to right and in uv spectrum started from left to right
why we use glass fiber filters use in some situation?
How do we get end points and how many end points are possible for citric acid and di-acid not theorotically answer should be given practically.
How we performed the force degradation for drug substance, is any specific guideline is available for each parameter(Acidic, basic, oxidation,heat)? what conditions you mentained for above parameters.
in monograph 7 imp are there but in vendor showing 5 imp do not req to include 2 imp for that what will be justification?
What is the principle of Thermal conductivity detector and FID?
A ha tc is actual defination of retention time?
if instrument calibration fails then what require to do?
In BP2013, Loperamid HCl monograph. Assay by titration with 0.1N sodium hydroxide using hydrocloric acid 0.01N and reading the volume added between the 2 points of inflexion. I have a question that if the diluent solvent is ethanol is certainly consumed a amount of volume of titrant, so this volume must be eliminated on the result calculation or not apart from first point which is subtracted above.
what is lod and loq ?,why use k2cr2o7 , kcl h2so4 in uv calibration ?,why use benzophenone & caffene acetone in hplc calibration ?,what is leading peak in hplc ?why we do the calibration of limit of stry light in hplc & uv ?
Loss of linearity in tkn analysis, possible reasons?
