we run the same sample in same method in different flow rates
in HPLC,any changes in sample analysis?
Answer Posted / uvreddy
changes are there,because flow rate increases closely peaks
will merge,flow rate decreses some time closely peaks will
come better resolution.
| Is This Answer Correct ? | 12 Yes | 1 No |
Post New Answer View All Answers
In HPLC Calibration, On which basis RSD Limit of noise test is fixed (NMT 33.0 % )
In Dissolution Test why limit is define Q+5% what is the role of +5%.
How we performed the force degradation for drug substance, is any specific guideline is available for each parameter(Acidic, basic, oxidation,heat)? what conditions you mentained for above parameters.
My question about gas chromatography sulfur chemiluminsecence detector. I test unknown sample gas by GC-SCD (calibrated ) and the result of *H2S is 279 PPM , *but when I test the same sample with the GC-TCD (calibrated ) the value of *H2S is 2500 PPM . I'd like to inform you that both GCs are calibrated and have very good operation conditions with stable parameters . the question is if the sample gas with higher H2S over detection limits of SCD detector (1000 ppm). why the result it 279 ppm Best regards
[3/28, 20:52] Manoj P Venkatpurwar: how many impurities require to inject in assay specificity that how we can find out? and in Rs also how?
Why six unit used for precision?
why we should take dst factor for below 1%moisture samples
A ha tc is actual defination of retention time?
Did anybody have method for acetyl cysteine effervescnce tablet
which are the diffrent batches in the pharmaceuticals?
In GC calibration,what is the procedure to calibrate the TCD (thermal counductivity detector)suggest ?
identification is for unknown? qualification for known? reporting for LOQ?
4. Describe the operation of the Craig apparatus. Chapter.3 Equilibrium Processes in Separations
in which situation ion pair require to use?
Which parameter require to do for analytical method equivalency?